Doctor of Philosophy, Case Western Reserve University, 2012, Materials Science and Engineering
This dissertation explores the development of a new stainless steel pressure sensor capable of sustaining harsh environments, including high pressures, high temperatures, and/or corrosive media. The proposed pressure sensor utilizes commercial off-the-shelf (COTS) components, adapts vacuum coupling radiation (VCR) tube fitting (Swagelok Co.) for sensor packaging, and combines micro- and conventional-machining techniques for sensor realization. Capacitive transduction is used to simplify the implementation, as well as take advantage of the high stability and low temperature drift associated with this transduction scheme. Two generations of stainless steel capacitive pressure sensors have been developed in this dissertation.
The first-generation sensor is comprised of a stainless steel diaphragm die and a stainless steel backing plate, each electrically isolated with tetraethylorthosilicate (TEOS) silicon dioxide, and packaged by a set of COTS VCR tube fitting. The pressure sensor responses show four operating regions, including stabilizing, non-touch, transition, and touch mode regions. The fully packaged pressure sensor is characterized at high pressures of up to 10,340 kPa (1,500 psi) and at high temperatures of up to 300°C. Corrosive pressure media, including potassium hydroxide (KOH) and tetramethylammonium hydroxide (TMAH) solutions, are used to demonstrate the corrosive-media compatibility of the pressure sensor. After soaking in these corrosive media and several tens of pressure cycles over a month, the fully packaged pressure sensor continues to show stable and consistent operation. Because of the anomalous stabilizing region in these sensors, sensor-to-sensor variance is very poor (i.e., 62% in full-scale (FS)).
The second-generation sensor is developed to address the shortcomings found in the first-generation pressure sensor. A hard tungsten carbide backing plate used to replace the stainless steel backing plate and a stainless steel press plate are used (open full item for complete abstract)
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Committee: Mehran Mehregany (Advisor); Frank Ernst (Committee Member); Pirouz Pirouz (Committee Member); Harold Kahn (Committee Member)
Subjects: Engineering