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KW Thesis 06132014 Final NO SIG 2.pdf (4.46 MB)
ETD Abstract Container
Abstract Header
The Synthesis of Polyimides Containing Oxyalkylene Units
Author Info
Wickman, Kristy
Permalink:
http://rave.ohiolink.edu/etdc/view?acc_num=wright1405623715
Abstract Details
Year and Degree
2014, Master of Science (MS), Wright State University, Chemistry.
Abstract
A series of oxyalkylene containing diamines, 1,4-bis(2-(4-aminophenoxy)-ethoxy)benzene, 2,2-bis[4-(2-(4-nitrophenoxy)ethoxy)phenyl]hexafluoropropane, 9,9-bis(4-(2-(4-nitrophenoxy)ethoxy)phenyl)fluorene, and bis(4-(2-(4-nitrophenoxy)ethoxy)-phenyl)diphenylmethane, has been synthesized from the reduction of 1,4-bis(2-(4-nitrophenoxy)ethoxy)benzene, 2,2-bis[4-(2-(4-nitrophenoxy)ethoxy)phenyl]-hexafluoropropane, 9,9-bis(4-(2-(4-nitrophenoxy)ethoxy)phenyl)fluorene, bis(4-(2-(4-nitrophenoxy)ethoxy)phenyl)diphenylmethane, respectively. The diamine compounds were reacted reacted with 6FDA to obtain the corresponding polyimide. The polymerization was done in a one-pot reaction with m-cresol and isoquinoline. The polyimides displayed glass transition temperatures ranging from 186-231°C and thermal stability >400°C.
Committee
William Feld, Ph.D. (Advisor)
Eric Fossum, Ph.D. (Committee Member)
David Grossie, Ph.D. (Committee Member)
Pages
71 p.
Subject Headings
Chemistry
Keywords
polymer
;
polyimide
;
diamines
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Citations
Wickman, K. (2014).
The Synthesis of Polyimides Containing Oxyalkylene Units
[Master's thesis, Wright State University]. OhioLINK Electronic Theses and Dissertations Center. http://rave.ohiolink.edu/etdc/view?acc_num=wright1405623715
APA Style (7th edition)
Wickman, Kristy.
The Synthesis of Polyimides Containing Oxyalkylene Units.
2014. Wright State University, Master's thesis.
OhioLINK Electronic Theses and Dissertations Center
, http://rave.ohiolink.edu/etdc/view?acc_num=wright1405623715.
MLA Style (8th edition)
Wickman, Kristy. "The Synthesis of Polyimides Containing Oxyalkylene Units." Master's thesis, Wright State University, 2014. http://rave.ohiolink.edu/etdc/view?acc_num=wright1405623715
Chicago Manual of Style (17th edition)
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Document number:
wright1405623715
Download Count:
537
Copyright Info
© 2014, all rights reserved.
This open access ETD is published by Wright State University and OhioLINK.